Synthesis, Spectroscopic, Thermodynamic and Biological Activity Studies of Schiff Base and Metal Complexes Derived From 2-[ 1H-Pyrrol-2-Ylimino Methyl]- 5-Phenyl-1,3,4- Oxadiazole
schiff base, microwave synthesis, thermodynamic parameters, biological activity
Abstract
New metal complexes of the ligand (HL) 2-[1H-Pyrrol-2-ylimino methyl]-5-phenyl-1, 3,4-oxadiazol with the metal ions Co(II), Ni(II) and Cu(II), were prepared in alcoholic medium. The Schiff bases were condensed by using [Pyrrolcarboxaldehyde] with[2-amino-5-(phenyl-1, 3,4-oxadiazole] in alcoholice medium. As the Schiff baseprepared was tridentate ligand, it was used for forming complexes with Co+2, Ni+2, Cu +2 and Zn+2 ions of type M (HL)2. All the synthesized Schiff base and their metal complexes were characterized by FTIR Spectroscopy, Electronic Spectroscopy, Elemental Analysis,
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References
M. Farah, A. Pilotti 11(3-4), 3-4.
B. Waston, J. Tierney, P. Lidstrom (2002) 6, 373-380.
Kidwai M, Kumar P, Goel Y, Ind. Chem (1997) 36B, 175-179.
K. Khan, M. Rani, S. Haider Khan K.M., Rani M. and Haider S.M., Lett.
K. Joshi, H. Dabhi, A. Pancholi, A. Rana (1996) Ligand field parameters of Cu (II), Ni (II) and Co (II) chelates with some 4-substituted-1-phenyl-3- methyl-2-pyrazolin-5-ones. 12(3), 287-290.
Y. Emad, A. Hadeel, M. Farah (2010) Synthesis and characterization of some metal ions with 2-amino acetate benzothiazol. 6(7), 879-882.
A. Coats, J. Redfern (1964) Kinetic Parameters from Thermogravimetric Data. 201(4914), 68-69. https://doi.org/10.1038/201068a0
H. Horovitz, G. Metzger (1963) Analysis of thermogravimetric traces as an approach to determine the mechanism of dissociation of copper (II)-α-aryl azoacetoacetylaminopyridine chelates. 159, 43-54.
A. Johnsoa, Wilcox (1969) Lab. Exp. Org. Chem. 219.
Chudgar, S. N.K; Shan, R. Vorat (1989) Mesogenic Semicarbazones and Amino Oxadiazoles-I. 172, 51-56.
R. Sliverstien, G. Bassler, T. Morrill (2005) Spectrometric Identification of Organic Compounds. 7th addition.
NakamotoK (1963) Infrared spectra of Inorganic and coordination Compounds.
D. Adans (1967) Metal-Ligand and related Vibration. 310.
Rahman F, Ahmad J, Haq M (2009) Tris- (salicylaldehyde)-complexes. 4(4), 229-234.
K. Sahoo, P. Das, S. Nayak (1973) Synthesis and Characterization of Some Cobalt. 1011.
R. Sarika, R. Amit, B. Gaurav, S. Anand (2003) Synthesis and characterization of transition metal complexes with N, O-chelating Hydrazone Schiff base ligand", American-Eurasian Complexes Containing Heterocyclic Nitrogen Donor Ligands. 91-96.
Manish srivastava, Deepak Singh, Aashishsinghkushwah, P. Gokulan (2010) 04, 20-24.
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